G
Graeme
Calibration procedures and metrological measurements are supposed to be based on authoritative references ... but what do you do when several references have conflicting information? I have recently seen an example of this, and I would like to throw it out for discussion.
A technician was calibrating a digital temperature indicator that can use either J or K thermocouples. The calibration method applies a DC voltage to the meter inputs to simulate a thermocouple. This technician is still new in the lab and is eager to learn, so she has been studying a lot - even reading some of the stuff I write! Her diligent study has prompted a question. We have already fixed the potential problem in our process, but the fundamental question remains.
(Note: all temperatures listed are in degrees Celsius.)
The manufacturer specification for the meter covers almost the full range of the NIST emf tables for a J thermocouple: -200 to 760 degrees. There are accuracy limits specified over this entire range: ±(0.1% reading + 1.2 deg). We also calibrate similar meters with even tighter specifications: ±(0.05% reading + 0.6 deg). The question relates to the fact there is little agreement among the references we have available about the usable range of the Type J thermocouple, and about the existence or magnitude of error limits.
To me, the net effect of these conflicting sources seems to be that if your stick a J thermocouple probe into something colder than the ice point, you will get an indication on the meter but it may or may not have any meaning. This leads to the question our technician raised – if a meter is outside its specification range at a point (for example, -100 deg), then is it really "out of tolerance"?
Have you seen this type of problem? How would you handle it? (Don’t cheat by reading the final paragraph to see what we have done for now.)
References
We have addressed the situation by changing the calibration procedure so that J thermocouple inputs are not tested below the ice point. This does not affect any of our current customers because all of them are measuring processes above 30 degrees.
A technician was calibrating a digital temperature indicator that can use either J or K thermocouples. The calibration method applies a DC voltage to the meter inputs to simulate a thermocouple. This technician is still new in the lab and is eager to learn, so she has been studying a lot - even reading some of the stuff I write! Her diligent study has prompted a question. We have already fixed the potential problem in our process, but the fundamental question remains.
(Note: all temperatures listed are in degrees Celsius.)
The manufacturer specification for the meter covers almost the full range of the NIST emf tables for a J thermocouple: -200 to 760 degrees. There are accuracy limits specified over this entire range: ±(0.1% reading + 1.2 deg). We also calibrate similar meters with even tighter specifications: ±(0.05% reading + 0.6 deg). The question relates to the fact there is little agreement among the references we have available about the usable range of the Type J thermocouple, and about the existence or magnitude of error limits.
- The NIST web site (see the references, below) has emf vs. temperature tables that go down to -210 degrees. These tables are reproduced in the other references.
- The book by Nicholas & White, and the Omega reference section in their catalog, have a note stating that J thermocouples "should not be used at low temperatures". Neither source defines what "low" means.
- The ASTM manual states that J thermocouples "should not be used below the ice point". (0.00 degrees)
- The ASTM manual also states that there are no established limits of error for J thermocouples below the ice point.
- The table in Nicholas & White has limit of error specifications, but only down to -40 deg.
- The table in the Omega reference has limit of error specifications for the entire range.
- The NIST table has nothing on limits of error.
To me, the net effect of these conflicting sources seems to be that if your stick a J thermocouple probe into something colder than the ice point, you will get an indication on the meter but it may or may not have any meaning. This leads to the question our technician raised – if a meter is outside its specification range at a point (for example, -100 deg), then is it really "out of tolerance"?
Have you seen this type of problem? How would you handle it? (Don’t cheat by reading the final paragraph to see what we have done for now.)
References
- ASTM: Manual on the use of thermocouples in temperature measurement, 4th edition. ASTM, 1993.
- Nicholas & White: Traceable Temperatures, 2nd Edition. Wiley, 2001.
- NIST: ITS-90 Thermocouple Database (http://srdata.nist.gov/its90/main/)
- Omega Engineering: Temperature reference section (http://www.omega.com/temperature/Z/zsection.asp)
We have addressed the situation by changing the calibration procedure so that J thermocouple inputs are not tested below the ice point. This does not affect any of our current customers because all of them are measuring processes above 30 degrees.